VALWAVEfeQuKTA V®» S&Gs 1'2& lg&42&, 1*28, 129, 1-3J, 132, ^1l&^ 13^1|LtlMK *73%*78, 179, and 18Jr ! CAMP EDWARDS IMPACT ARIA GROUNDWATER STUDY MASSACHUSETTS MILITARY RESERVATION CAPE COD, MASSACHUSETTS Prepared for NATIONAL GUARD BUREAU ARLINGTON, VIRGINIA Prepared by OGDEN ENVIRONMENTAL AND ENERGY SERVICES 239 Littleton Road, Suite %B Westford, Massachusetts 01886 ^pnfpmhpr 1000 Digitized by the Internet Archive 2013 in http://archive.org/details/validateddatafor122unse > VALIDATED DATA FOR SDGs 122, 124-126, 128, 129, 131, 132, 134, 137, 153-156, 161, 162, 165, 173, 178, 179, and 181 OF THE CAMP EDWARDS IMPACT AREA GROUNDWATER STUDY MASSACHUSETTS MILITARY RESERVATION CAPE COD, MASSACHUSETTS Prepared for NATIONAL GUARD BUREAU ARLINGTON, VIRGINIA Prepared by OGDEN ENVIRONMENTAL AND ENERGY SERVICES 239 Littleton Road, Suite IB Westford, Massachusetts 01886 September 1999 TABLE OF CONTENTS Group Analytical Matrix EPA Method Database Reference Pages Group A Explosives Air 8330 833ON 1-2 B Explosives Profile 8330 833ON 1-39 C Explosives Soil 8330 833ON 1-27 D Volatiles Water OLC02.1 OC21V 504-EDB 504 8021-MTBE 8021W E Volatiles Profile OLC02.1 OLC02.1 1-78 F Volatiles Soil OLM03.2 OM31V 1-46 8021-EDB, 802IS MTBE G Semivolatiles Water OLC02.1 OC21B H Semivolatiles Soil OLM03.2 OM31B 1-60 I Pesticides/ Water OLC02.1/8151 OL21P/8151 Herbicides J Pesticides/ Soil OLM03.2/8151 OM31P/8151 1-38 Herbicides K Metals/Wet Water ILM04.0 Various Chemistry L Metals/Wet Soil ILM04.0 Various 1-34 Chemistry * No samples scheduled for EPA method/matrix September 1999 DATA QUALIFIER REFERENCE TABLE Qualifier Organics Inorganics U The analyte was analyzed for, but was not The material was analyzed for, butwas not detected abovethe reported sample quantitation detected above the level ofthe associated limit. value. The associatedvalue is eitherthe sample quantitation limit orthe sample detection limit J The analyte was positively identified; the The associated value is an estimated associated numerical value is the approximate quantity. concentration ofthe analyte in the sample. N The analysis indicates the presence ofan analyte Not applicable. forwhichthere is presumptive evidence to make a "tentative identification." NJ The analysis indicates the presence ofan analyte Not applicable. thathas been "tentatively identified" andthe associated numerical value represents its approximate concentration. UJ The analyte was not deemed above the reported The material was analyzedfor, butwas not sample quantitation limit. However, the detected. The associated value is an estimate reported quantitation limit is approximate and and may be inaccurate or imprecise. may ormay notrepresentthe actual limit of quantitation necessary to accurately and precisely measure the analyte in the sample. R The sample results are rejected dueto serious The data are unusable. (Note: Analyte may deficiencies in the ability to analyze the sample ormay notbe present). andto meet quality control criteria. The presence or absence ofthe analyte cannotbe verified. * V September 1999 QUALIFICATION CODE REFERENCE TABLE Qualifier Organics Inorganics H Holdingtimes were exceeded. Holdingtimeswere exceeded. S Surrogate recoverywas outside QC limits. The sequence ornumberofstandards usedfor the calibrationwas incorrect. c Calibration%RSD or%Dwere noncompliant. Correlationcoefficient is <0.995. R Calibration RRFwas <0.05. %Rforcalibration is notwithin control limits. B Presumed contamination from preparation Presumed contamination from preparation (method) blank. (method) orcalibration blank. %R L Notapplicable. Laboratory Control Sample were notwithin control limits. Q MS/MSD recovery was pooror RPD high. MS recovery was poor. E Not applicable. Duplicates showed pooragreement. I Internal standardperformance was ICP ICS results were unsatisfactory. unsatisfactory. A Notapplicable. ICP Serial Dilution %D were notwithin control limits. M Tuning (BFB orDFTPP) was noncompliant. Notapplicable. T Presumed contamination from trip blank. Notapplicable. + False positive - reported compoundwas not Not applicable. present. - False negative - compound was present but not Notapplicable. reported. F Presumed contamination from FB orER. Presumed contamination from FB or ER. $ Reportedresult orother information was Reported resultorother information was incorrect. incorrect. ? TIC identity orreported retentiontime has been Not applicable. changed. D The analysis with this flag shouldnot be used The analysiswith this flag should not be used because anothermoretechnically sound because anothermoretechnically sound analysis is available. analysis is available. P Instrumentperformance for pesticideswas Post Digestion Spike recoverywas not within poor. control limits. *# Unusual problems found with the datathathave Unusual problems foundwiththe datathat have been described in Section 1, "DataValidation been described in Section 1, "Data Validation Findings." The numberfollowingthe asterisk Findings." The number followingthe asterisk (*) will indicatethe subsection where a (*)will indicate the subsection where a description ofthe problem can be found. description ofthe problem can be found. September 1999