DEVELOPING THE NEW HAYABUSA CURATION FACILITY AT JOHNSON SPACE CENTER. B. T. De Gregorio1, M. E. Zolensky2, R. Bastien1, B. McCann1, D. R. Frank1, J. L. Warren1, and C. C. Allen2, 1ESCG/NASA Johnson Space Center (e-mail: [email protected]), 2NASA Johnson Space Center (e- mail: [email protected]). Introduction: On 25 November 2005 the Japan rials embedded in its upper surface. Unfortunately the Aerospace Exploration Agency (JAXA) Hayabusa use of anodized aluminum was necessary in the con- spacecraft made contact with the asteroid 25143 Ito- struction of the clean room frame (visible in Figure 1) kawa and collected a small amount of regolith dust to strengthen it and eliminate corrosion and wear over from Muses Sea region of smooth terrain [1]. Even time. All anodized aluminum interior to the lab will be though optimal sample collection did not occur, the covered by clean room tape or replaced with new stain- spacecraft returned to Earth with more than 10,000 less steel parts. We note that this is a problem shared grains ranging in the size from 30-180 μm [2]. These by almost all clean rooms. grains represent the only collection of pristine material Manipulating Sub-mm Asteroid Grains: Al- returned from an asteroid by a spacecraft. As part of though NASA already curates two other collections the joint agreement between JAXA and NASA for the containing sub-mm extraterrestrial particles, these mission, 10% of the Hayabusa grains will be trans- ferred to NASA for parallel curation and allocation, the first 15 of which arrived in December 2011. In order to properly receive and process these samples, a new cu- ration facility was developed at Johnson Space Center (JSC). Creating a Pristine Curation Environment: Since the Hayabusa samples within the JAXA curation facility have been stored and processed in specially- designed cabinets, free from exposure to terrestrial atmosphere and contamination [3], one of the goals of the new NASA curation facility was to continue this requirement. An unused lab space at JSC was trans- formed into a 120 sq.ft. ISO class 4 (equivalent to the original class 10 standard) clean room. Hayabusa sam- ples will be stored, observed, processed, and packaged for allocation inside a stainless steel glove box under dry N (Figure 1). Construction of the clean laboratory 2 was completed in December 2011 and an internal “op- erational readiness inspection” (ORI) is underway in order to confirm that the lab meets the NASA cleanli- ness and contamination control requirements for sam- ple curation. Currently, the first batch of 15 Hayabusa particles transferred to NASA are being stored by themselves in a clean-room cabinet in the Cosmic Dust Laboratory until the Hayabusa Lab is fully operational. Special care has been taken to remove or contain materials that may contribute contaminant particles in the same size range as the Hayabusa grains, which range up to 300 μm but are predominantly less than 10 μm in diameter. Several witness plates of various ma- terials will be installed around the clean lab and within the glove box to identify local contaminants at regular FIGURE 1. The new Hayabusa clean lab and sample cabinet at JSC, intervals by SEM and mass mpectrometry. Of particu- after construction has been completed but before ORI clearance. A lar interest is anodized aluminum, which contains co- new glass front for the glove box will be fabricated, and any ano- pious sub-mm grains of a multitude of different mate- dized aluminum parts will be replaced with new stainless steel parts. collections include terrestrial materials that significant- Allocation of NASA’s Hayabusa Samples: The ly aid in their manipulation by sharp glass needles. For first JAXA international Announcement of Opportuni- example, Cosmic Dust particles and aggregates contain ty (AO) for Hayabusa samples is scheduled for January a thin layer of silicone oil that helps them attach to the 2012, and NASA’s AO announcement will be syn- needle tip, while Stardust cometary grains are sur- chronized with it. The first sample allocations of rounded by silica aerogel. In contrast, the Hayabusa NASA materials should occur sometime during Sum- asteroid grains are “naked”, and some other form of mer 2012. The entirety of NASA’s allotment of Haya- assistance is required. busa grains will be available to both domestic and in- JAXA/ISAS and researchers at Kyushu University ternational researchers. The first 15 Hayabusa particles and Sendai University, under the direction of Tomoki will be allocated “as is”, without processing. However, Nakamura and Akio Fujimura have developed a elec- future grains can be allocated in a variety of processed trostatic particle manipulator system, which we are states, as requested by researchers. Preliminary exami- now adapting to our lab (Figure 2). In general, this nation of the first 15 Hayabusa particles by low voltage system operates by establishing a constant residual SEM/EDS has been performed at the JAXA curation charge on the probe needle, which attracts the particle facility, and many of the future grains transferred to to be transported. Removing or neutralizing the charge NASA will also be characterized in this way, either at allows the particle to be set down. A prototype system JAXA or at JSC. However, a subset of future NASA has been successfully tested with sub-mm grains of curated grains will likely remain pristine and uncharac- San Carlos olivine. The electrostatic manipulator sys- terized. It should be noted, however, that many of tem will be incorporated with an optical microscope these uncharacterized grains will be composed of alu- and micro-manipulator controls similar to the setups minum from the walls of the sample catcher. Addition- used in the Cosmic Dust and Stardust curation facili- al information about NASA’s Hayabusa collection, ties. The entire microscope/micro-manipulator setup curation, and allocation is available at will be placed inside the glove box and controlled by a http://curator.jsc.nasa.gov/hayabusa/. curator in the clean lab through the glove ports. It will be non-trivial to adapt this system for such use. Alter- References: [1] Yano H. et al. (2006) Science, 312, natively, we are testing the efficacy of a “vacuum 1350. [2] Nakamura T. et al. (2011) Science, 333, tweezer” system using quartz glass needles with an 1113. [3] Yada T. et al. (2011) Meteoritics & Planeta- open tip diameter less than 5 μm. However, such a ry Science, 74 (suppl.), abstract 5386. vacuum system would necessarily be located outside of the glove box. FIGURE 2. Prototype of the voltage-assisted micro-manipulator system to be used to handle and transfer sub-mm asteroid grains. It has been operated successfully to manipulate olivine test grains in this size range.