इंटरनेट मानक Disclosure to Promote the Right To Information Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public. “जान1 का अ+धकार, जी1 का अ+धकार” “प0रा1 को छोड न’ 5 तरफ” Mazdoor Kisan Shakti Sangathan Jawaharlal Nehru “The Right to Information, The Right to Live” “Step Out From the Old to the New” IS 13784 (1993): Pesticide - Dodine, Technical [FAD 1: Pesticides and Pesticides Residue Analysis] “!ान $ एक न’ भारत का +नम-ण” Satyanarayan Gangaram Pitroda ““IInnvveenntt aa NNeeww IInnddiiaa UUssiinngg KKnnoowwlleeddggee”” “!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता हहहहै””ै” Bhartṛhari—Nītiśatakam “Knowledge is such a treasure which cannot be stolen” Indian Standard PESTICIDE - DODINE, TECHNICAL - SPECIFICATION CDU 632’952 DOD I@ SIB 1993 BUREAU OF INDIAN STANDARDS KANAM ,NAVAHB 9 RUDAHAB HAHS RAFAZ GRAM WEN IHLED 110002 ,May 3991 Price Group 1 sedicitseP lanoitceS ,eettimmoC FAD 1 FOREWORD This naidnI dradnatS was detpoda yb eht uaeruB fo naidnI Standards, retfa eht tfard dezilanif ,yb the sedicitseP lanoitceS eettimmoC had neeb devorppa yb eht dooF and erutlucirgA noisiviD .licnuoC ,enidoD lacinhcet is deyolpme ni eht noitaraperp fo ladicignuf .snoitalumrof enidoD is eht desoporp nommoc eman yb eht lanoitarretnI noitazinagrO rof noitazidradnatS ( 0SI ) rof enidinauglycedod .etateca ehT laciripme and larutcurts ealumrof and ralucelom mass, of enidod era nevig :woleb Empirical Formula Structural Formula Molecular Mass @ G&hnN& / Y”’ 287’4 CH3-(CH2)jj-NH- c---NH2-CH3~~f in the noitaraperp fo this standard, eud noitaredisnoc has neeb nevig ot eht snoisivorp fo .eht sedicitcesnI Act, 1968 and eht seluR demarf .rednuereht ,rewewoH this standard is detcejbus ot the snoitcirtser desopmi rednu eht Act and seluR reverehw .elbacilppa roF eht esoprup fo gnidiced rehtehw a ralucitrap tnemeriuqer fo this standard is deilpmoc htiw eht lanif ,eulav ,devresbo ro ,detaluclac gnisserpxe eht tluser fo a tset ro ,sisylana shall eb .dednuor ffo ni ecnadrocca htiw SI 2 : 1960 seluR‘ rof gnidnuor ffo laciremun seulav ( revised )‘. The. number fo tnacifingis secalp deniater ni eht dednuor ffo eulav dluohs eb eht emas as that fo eht specified eulav ni this standard. . .“. ..“^ . . IS 13784: 1993 Indian Standard PESTICIDE - DODINE, TECHNICAL - SPECIFICATION 1 SCOPE Insecticides Act, 1968 dna seluR demarf -ereht :rednu sihT dradnats sebircserp the stnemeriuqer dna a) emaN of the ;lairetam the sdohtem of gnilpmas dna test for ,enidod .lacinhcet )b emaN of the ;rerutcafunam Date of ;erutcafunam C) 2 SECNEREFER d) Batch ;rebmun ehT naidnI sdradnatS detsil woleb are yrassecen e) enidoD ,tnetnoc per&t ( m/m ); stcnujda ot siht .dradnats f) Net ssam of the ;stnetnoc dna IS No. Title g) ehT muminim yranoituac eciton as 1070 : 1992 tnegPeR grade water ( driht worded ni the Insecticides Act, 1968 dna seluR demarf .rednuereht revision ) 6940 : 1982 Methods of test for sedicitsep Table 1 Requirements for Dodine, Technical dna rieht snoitalumrof (Jirst ( Clause 3.2 ) revision ) 8069 : 1989 hgiH ytisned enelyhteylop S1 citsiretcarahC tnemeriuqeR Method of Test, Ref to ( HDPE ) nevow sacks for No. r____h____7 gnikcap sedicitsep ( second xennA sihT fo SI lC6940 .oN : 1982: fo revision ) dradnatS 8190 stnemeriuqeR for gnikcap of (1) (2) (3) (4) (5) ( Part 1 ) : 1988 sedicitsep : Part 1 diloS )i enidoD ,tnetnoc 98 A - tnecrep yb ,ssam sedicitsep ( lrnocrs revision ) lliM 10946 : 1984 Methods of gnilpmas for )ii retaW ,tnetnoc 10 - 4.2 lacinhcet grade sedicitsep tnecrep yb ,ssam M0.Y )iii vtinil~~klA ( sa 005 - 11.3.2 3 REQUIREMENTS NaOH ) tnecrep 3.1 noitpircseD yb ,ssam Max OK ytidicA ( s,2 0.05 - 11.3.2 ehT lairetam llahs eb ni the mrof of etihw ot off ,OSLH ) tnecrep etihw enillatsyrc powder free morf hard ,spmul yb ,wm Max suoenartxe seitirupmi of added gniyfidom .)s(tnega 6 SAMPLING 3.2 ehT lairetam llahs ylpmoc htiw the -eriuqer stnem nevig ni elbaT 1. evitatneserpeR selpmas of the lairetam llahs eb nward gnidrocca ot 1s 10946 : 1984. 4 GNIKCAP 7 TESTS ehT lairetam llahs eb packed ni erbif draob smurd denil htiw LDPE of ssenkciht ton ssel 7.1 stseT llahs cb deirrac tuo yb the sdohtem naht 0‘125 mm or HDPE nevow sacks detanimal referred ot ni co1 4 dna 5 of the elbaT .1 htiw 0’025 mm LDPE [ see SI 8069 : 1989 1. ehT lareneg stnemeriuqer nevig ni SI 8190 ( Part 1 > : 7.2 Quality of Reagents 1988 llahs eb .dewollof sselnU deificeps ,csiwrchto c-IUG slacintehc dna 5 GNIKRAM dellitsid water ( :tes SI 1070 : 1992 ) llahs eb deyolpme ni tests. ehT reriatnoc llahs raeb ylbigel dna ylbiledni NOTE - eruP‘ ’slacimehc llahs naem slacimehc the gniwollof noitamrofni ni noitidda ot yna tl:ht od ton niatnoc sertirlipmi hcihw tcefz eht other noitamrofni as si yrassecen rednu the stluser fo .sisylana IS 13784 : 1993 ANNEX A [ Clause 3.2, Table 1, Item )i( ] NOITANIMRETED FO ENIDOD TNETNOC A-l ELPICNIRP erehw V1 = ,emulov ni ,lm fo standard enidoD is devlossid ni citeca dica citeca- cirolhcrep dica deriuqer rof eht edirdyhna tnegaer ot ecudorp a noitulos fo eht noitartit rof eht ;elpmas dnuopmoc that is cisab hguone ot eb elbartit htiw cirolhcrep dica using latsyrc teloiv as an ,v = ,emulov ni ,lm fo standard .rotacidni cirolhcrep dica deriuqer rof blank ;noitanimreted 2-A STNEGAER N = ytilamron fo standard cirolhcrep ;dica and 1.2-A citecA dicA - laicalg suordyhna M- mass, ni g, fo eht elpmas nekat rof eht .tset 2.2-A citecA edirdyhnA 3.2-A latsyrC teloiV rotacidnI - 1’0 tnecrep 5-A NOITAZIDRADNATS FO CIROLHCREP ( m/v ) ni citeca .dica ACID 4.2-A cirolbcreP dicA - 1’0 N. 1.5-A erudecorP evlossiD 5’8 lm fo 70 tnecrep cirolhcrep dica ni oT 900 lm laicalg citeca dica at tuoba 25°C add laicalg citeca .dica Add 15 lm citeca edirdyhna 2’8 lm fo cirolhcrep dica ( 72 tnecrep w/w ,) .xim ylsuoituac and ekam up ot 1000 .lm peeK Add 32 lm fo citeca ,edirdyhna and again .xim .thginrevo looC ot moor ,erutarepmet ekam up eht emulov ot 1000 lm htiw laicalg citeca .dica ezidradnatS 3-A PROCEDURE eht detulid c:rolhcrep dica against OO:.o g muissatop negordyh ,etalahthp hcihw has neeb 1.3-A hgieW yletarucca tuoba 6’0 g fo lacinhcet deird ot tnatsnoc thgiew at 120°C erofeb elpmas and refsnart ylevitatitnauq otni a lm-052 .gnihgiew evlossiD eht muissatop negordyh reyemnelrE .ksalf Add 90 lm citeca edirdyhna etalahthp ni 70 lm citeca dica no a htab-retaw and 10 lm laicalg clteca .dica Warm eht stnetnoc tuoba( 20 setunim .) Add 30 lm fo citeca ,dica at 50 - 70°C no a retaw bath rof 5 setunim rof net spord fo latsyrc teloiv as .rotacidni etartiT etelpmoc .noitulossid looC eht stnetnoc fo eht htiw detulid cirolhcrep .dica ehT dne tniop is ksalf ot moor .erutarepmet detacidni yb eht egnahc fo ruoloc fo eht stnetnoc fo eht ksalf morf teloiv ot .eulb etaluclaC eht rtartiT eht stnetnoc against 1’0 N cirolhcrep ytilamron ( )N using eht gniwollof :alumrof dica using latsyrc teloiv .rotacidni ehT tniop is detacidni yb eht egnahc fo ruoloc fo eht stnetnoc 2.S-A noitaluclaC fo eht ksalf morf teloiv ot .eulb ytilamroN ( )N = v- _“~(‘2~J~22~j 2.3-A yrraC tuo a blank noitanimreted htiw erehw 90 lm citeca edirdyhna and 10 lm citeca dica m = mass, ni g, fo muissatop negordyh using latsyrc teloiv as an .rotacidni ;etalahthp 4-A NOITALUCLAC V = ,emulov ni ,lm fo cirolhcrep dica ;demusnoc and enidoD ,tnetnoc M = ralucelom thgiew fo muissatop percent by mass ~-28'~~ ' ( vI - '2 ) x_fi M negordyh etalahthp ( 22’402 .)‘ 2 dradnatG Mark ehT esu fo eht dradnatS Mark is denrevog yb eht snoisivorp fo eht Bureau of Indian Standards Acf, 1986 and eht seluR and snoitalugeR edam .rednuereht ehT dradnatS Mark no stcudorp derevoc yb an naidnI dradnatS syevnoc eht ecnarussa that yeht evah neeb decudorp ot ylpmoc htiw eht stnemeriuqer fo that standard rednu a llew denifed metsys fo ,noitcepsni gnitset and ytilauq lortnoc hcihw is desived and desivrepus yb SIB and detarepo yb eht -orp .recud dradnatS dekram stcudorp era osla ylsuounitnoc dekcehc yb SIB rof ytimrofnoc ot that standard as a rehtruf .draugefas sliateD fo snoitidnoc rednu hcihw a ecnecil rof eht esu fo eht dradnatS Mark yam eb detnarg ot srerutcafunam ro srecudorp yam eb morf-deniatbo eht uaeruB fo naidnI Standards. Bureau of Indian Standards SIB is a yrotutats noitutitsni dehsilbatse rednu eht ot etomorp Bureau of Indian Standards Act, 1986 suoinomrah tnempoleved fo eht seitivitca fo ,noitazidradnats gnikram and ytilauq noitacifitrec fo sdoog: and gnidnetta ot detcennoc srettam ni eht .yrtnuoc Copyright BIS has eht thgirypoc fo all its .snoitacilbup oN trap fo eseht snoitacilbup yam eb decudorper ni yna mrof tuohtiw eht roirp noissimrep ni gnitirw fo .SIB sihT seod ton edulcerp eht eerf ,esu ni eht esruoc fo gnitnemelpmi eht standard, fo yrassecen ,sliated hcus as slobmys and ,sezis sepyt ro edarg .snoitangised seiriuqnE gnitaler ot thgirypoc eb desserdda ot eht rotceriD ( snoitacilbuP ,) .SIB Review of Indian Standards stnemdnemA era issued ot standards as eht deen sesira no eht basts fo .stnemmoc Standards era osla deweiver ;yllacidoirep a standard gnola htiw stnemdnema is demriffaer nehw hcus weiver setacidni that on segnahc era ;dedeen fi eht weiver setacidni that segnahc era ,dedeen ti is nekat up rof -er .noisiv sresU fo naidnI Standards dluohs niatrecsa that yeht era ni noissessop fo eht tsetal -dnema stnem ro noitide yb gnirrefer ot eht tsetal issue fo SIB‘ ’koobdnaH and sdradnatS‘ ylhtnoM .’snoitiddA stnemmoC no this naidnI dradnatS yam eb tnes ot SIB gnivig eht gniwollof ecnerefer : toD : No. )911(lDAF Amendments Issued Since Publication dnemA .oN etaD fo eussI txeT detceffA UAERUB FO NAIDNI SDRADNATS :sretrauqdaeH Manak ,navahB 9 rudahaB Shah rafaZ Marg, weN thleD 110002 senohpeleT : 331 01 31, 331 13 75 smargeleT : Manaksanstha ( nommoC ot all seciffO ) lanoigeR :seciffO enohpeleT lartneC : Manak ,navahB 9 rudahaB Shah rafaZ Marg 331 01 31 WEN IHLED 110002 ( 331 13 7.5 nretsaE : 41/l C. .I .T emehcS IIV M, V. .I .P ,daoR alotkinaM 37 X4 99, 37 85 61 ATTUCLAC 700054 { 37 86 26, 37 86 62 53 38 43, 53 16 40 nrehtroN : SC0 ,644-544 rotceS 35-C, HRAGIDNAHC 160036 I 53 23 84 235 02 16, 235 04 42 nrehtuoS : C. .I .T Campus, VI ssorC ,daoR MADRAS 600113 t 235 15 19, 235 23 15 nretseW : ,ayalakanaM 9E MIDC, ,loraM irehdnA ( East ) 632 92 95, 632 78 58 YABMOB 400093 632 78 91, 632 78 92 sehcnarB : .DABADAMHA .EROLAGNAB .LAPOHB .RAWHSENABUHB .EROTABMIOC .DABADIRAF .DABAIZAHG .ITAHAWUG .DABAREDYH JAIPUR. .RUPNAK .WONKCUL .ANTAP .MARUPAHTNANAVURIHT