Appendix I Standard Operating Procedures and Standard Quality Procedures This page intentionally left blank U.S. Department of Energy Oakland Operations Office, Oakland, California FINAL STANDARD OPERATING PROCEDURES for the: Environmental Restoration/Waste Management Laboratory for Energy-Related Health Research (LEHR) University of California at Davis, California Prepared for: United States Department of Energy Oakland Operations Office 1301 Clay Street Oakland, California 95612-5208 Prepared by: Weiss Associates 5801 Christie Avenue, Suite 600 Emeryville, CA 94608-1827 DOE Oakland Operations Contract DE-AC03-96SF20686 FINAL STANDARD OPERATING PROCEDURES for the: Environmental Restoration/Waste Management Laboratory for Energy-Related Health Research (LEHR) University of California at Davis, California Prepared for: United States Department of Energy Oakland Operations Office 1301 Clay Street Oakland, California 95612-5208 Prepared by: Weiss Associates 5801 Christie Avenue, Suite 600 Emeryville, CA 94608-1827 DOE Oakland Operations Contract DE-AC03-96SF20686 Issued To: ___________________ Date: ______________ Copy No.: ________ (cid:1) Controlled (cid:2) Uncontrolled J:\DOE\4000\D3\SQ&OPS\WASOPS\SOP_TOC1299.DOC WEISS ASSOCIATES Project Number: 128-4000 Approvals Page FINAL STANDARD OPERATING PROCEDURES for the: Environmental Restoration/Waste Management Laboratory for Energy-Related Health Research (LEHR) University of California at Davis, California Prepared for: United States Department of Energy Oakland Operations Office 1301 Clay Street Oakland, California 95612-5208 Prepared by: Weiss Associates 5801 Christie Avenue, Suite 600 Emeryville, CA 94608-1827 October, 2010 Approved by: Date: Mary Stallard, R.G. Project Quality Assurance Manager Weiss Associates Approved by: Date: Robert O. Devany, R.G., C.H.G. Project Manager Weiss Associates Approved by: Date: Michael D. Dresen, R.G., C.H.G. Program Manager Weiss Associates J:\DOE\4000\D3\SQ&OPS\WASOPS\SOP_TOC1299.DOC WEISS ASSOCIATES Project Number: 128-4000 Standard Operating Procedures and Forms Table of Contents LEHR Environmental Restoration / Waste Management 12/10/99 DOE Contract No. DE-AC03-96SF20686 Page i of vi TABLE OF CONTENTS AND LOG OF REVISIONS STANDARD OPERATING PROCEDURES SOP No. Title Revision Date of No. Revision SOP 1.1 Chain-of-Custody 1 3/99 SOP 2.1 Sample Handling, Packaging and Shipping 2 12/99 SOP 3.1 Surface and Shallow Subsurface Soil Sampling 1 4/02 SOP 3.2 Subsurface Soil Sampling While Drilling 1 4/02 SOP 4.1 Compaction of Fill Material 0 3/98 SOP 5.1 Water Level Measurements in Monitoring Wells 0 3/98 SOP 5.2 Non-aqueous Phase Liquid Measurement in Monitoring 0 3/98 Wells SOP 6.1 Sampling Equipment and Well Material Decontamination 0 3/98 SOP 6.2 Drilling, Development and Heavy Equipment 0 3/98 Decontamination SOP 7.1 Surface and Subsurface Geophysics 0 3/98 SOP 8.1 Monitoring Well Installation 0 3/98 SOP 8.2 Monitoring Well Development 0 3/98 SOP 8.3 Bore Hole and Well Abandonment 0 3/98 SOP 9.1 Low Flow Ground Water Sampling with Dedicated Pumps 1 10/10 SOP 10.1 Soil Organic Vapor Sampling 0 3/98 SOP 10.2 Cone Penetration Testing and Hydropunch Ground Water 0 3/98 Sampling SOP 10.3 Sample Collection, Handling and Data Documentation for 0 6/98 Field Analysis Using Gamma Spectrometer and Beta Scintillation Dectector SOP 10.4 Radium-226 Analysis by Gamma Spectrometer 0 7/01 SOP 10.5 Strontium-90 Analysis by Beta Scintillation Sensor 3 7/01 SOP 11.1 Aquifer Testing 0 3/98 SOP 12.1 Soil Stockpiling 0 3/98 SOP 13.2 Ambient Air Monitoring 1 3/99 SOP 14.1 Hollow Stem Auger Drilling 0 3/98 SOP 14.2 Mud Rotary Drilling 0 3/98 SOP 14.3 Air Rotary Drilling 0 3/98 SOP 14.4 Dual Tube Percussion Drilling 0 3/98 SOP 15.1 Lithologic Logging 0 3/98 SOP 17.1 Sample Labeling 0 3/98 SOP 17.2 Sample Numbering 0 3/98 SOP 18.1 Field QC Sampling 0 3/98 J:\DOE\4000\D3\SQ&OPS\WASOPS\SOP_TOC1299.DOC WEISS ASSOCIATES Project Number: 128-4000 Standard Operating Procedures and Forms Table of Contents LEHR Environmental Restoration / Waste Management 12/10/99 DOE Contract No. DE-AC03-96SF20686 Page ii of vi SOP 19.1 On-Site Sample Storage 0 3/98 SOP 20.1 Sample Containers, Preservation, and Holding Times 0 3/98 SOP 21.1 Data Validation 1 10/10 SOP 21.2 Sample Data Management 0 10/10 SOP 23.1 Land Surveying 0 3/98 SOP 24.1 Radiological Areas and Postings[see RPP] 1 3/99 SOP 25.1 Radiological Surveys and Instrumentation [see RPP] 1 3/99 SOP 25.2 Radiological Survey Forms (Update 1) [see RPP] 0 7/98 SOP 29.1 Drum Crusher Operation and Servicing 0 3/98 SOP 30.1 Taskmaster Heavy Duty Solids Disintegrator (Shredder) 0 3/98 Operation and Servicing SOP 31.1 Lead Characterization, Packaging and Shipping 0 3/98 SOP 32.1 Contamination Control [see RPP] 1 3/99 SOP 34.1 Waste Processing and Packaging 0 7/98 SOP 34.2 Low-Level Radioactive Waste Storage 0 3/99 SOP 34.3 Waste Shipment 2 6/01 SOP 34.4 Clean Waste Handling 0 3/98 SOP 34.5 Waste Tracking System 0 2/99 SOP 35.1 Waste Certification 0 3/98 SOP 35.2 Waste Characterization for Off-Site Shipment 0 6/01 SOP 37.1 Tennelec Series 5 Low Background Counting System 0 3/99 [see RPP] SOP 37.2 Liquid Scintillation Counter (LSC) [see RPP] 0 3/99 SOP 38.1 Check-in and Orientation for Radiological Workers, 2 11/99 General Employees and Members of the Public [see RPP] SOP 38.2 External Dosimetry Issuance [see RPP] 2 11/99 SOP 38.3 Radiation Protection Records [see RPP] 2 11/99 SOP 38.4 Radiological Protection Program Audits [see RPP] 1 3/99 SOP 38.5 Occupational Exposure Reports [see RPP] 1 3/99 SOP 39.1 LEHR Site Inspection [see RPP] 1 3/99 SOP 40.1 Ambient Radiation Monitoring Program 0 4/98 SOP 41.1 LEHR Document Review Procedures 0 3/98 SOP 42.1 Environment, Safety and Health Reporting 0 9/01 SOP 43.1 Security 0 11/01 J:\DOE\4000\D3\SQ&OPS\WASOPS\SOP_TOC1299.DOC WEISS ASSOCIATES Project Number: 128-4000 Standard Operating Procedures and Forms Table of Contents LEHR Environmental Restoration / Waste Management 12/10/99 DOE Contract No. DE-AC03-96SF20686 Page iii of vi FORMS AND FIGURES FOR STANDARD OPERATING PROCEDURES SOP No. Form No. Form Title Revision Date of No. Revision SOP 1.1 Chain-of-Custody Record 1 3/99 Field Activity Daily Log 2 12/99 SOP 2.1 None SOP 3.1 Sample Collection Log 1 4/02 SOP 3.2 Borehole/Well Construction Log 0 3/98 SOP 4.1 None SOP 5.1 Water Levels Form 0 3/98 Well Development Data Form 0 3/98 Water Sampling Data Form 0 3/98 SOP 5.2 None SOP 6.1 None SOP 6.2 None SOP 7.1 None SOP 8.1 Borehole/Well Construction Log 0 3/98 SOP 8.2 Well Development Data Form 0 3/98 SOP 8.3 DWR Form 188, Rev. 7-90 0 3/98 Well Abandonment Log 0 3/98 SOP 9.1 None SOP 10.1 None SOP 10.2 None SOP 10.3 Field Screening Samples and Analysis 0 6/98 Form SOP 11.1 None SOP 12.1 None SOP 13.2 Example Air Monitoring 0 4/98 Chain-of-Custody Air Sampling Station Meter Log 0 4/98 Radtrack Alpha Track 0 4/98 Chain-of-Custody SOP 14.1 None SOP 14.2 None SOP 14.3 None SOP 14.4 None SOP 15.1 Borehole/Well Construction Log 0 3/98 SOP 17.1 Example Sample Label 0 3/98 J:\DOE\4000\D3\SQ&OPS\WASOPS\SOP_TOC1299.DOC WEISS ASSOCIATES Project Number: 128-4000 Standard Operating Procedures and Forms Table of Contents LEHR Environmental Restoration / Waste Management 12/10/99 DOE Contract No. DE-AC03-96SF20686 Page iv of vi SOP 17.2 None SOP 18.1 None SOP 19.1 None SOP 20.1 Equipment Checklist 0 3/98 Table 1. Recommendations for Water 0 3/98 Samples Table 2. Recommendations for 0 3/98 Sediment/Soil Samples SOP 21.1 Validation of Organic Data by GC/MS 1 9/10 Analysis Validation of Organic Data by GC 1 9/10 Analysis Validation of Radiochemistry Data 0 1/98 Validation of Metals Data 1 9/10 Validation of Data from Wet Chemistry or 0 1/98 other Miscellaneous Analyses Data Validation Qualifier Definitions 0 1/98 LEHR Data Validation Summary 0 1/98 SOP 21.2 Data Reporting Form 1/98 SOP 23.1 Standards for Third-Order Plane Surveys 0 3/98 SOP 24.1 Surface Confirmation Values 0 6/99 Values for Establishing Sealed Radioactive 1 6/99 Source Accountability with Radioactive Material Posting and Labeling Requirements SOP 25.1 Radiological Survey Log Sheet 1 3/99 SOP 25.2 Radiological Survey Form 0 7/98 Radiological Survey Form Continuation 0 7/98 Sheet Radiological Survey Log Sheet 1 3/99 Radioactive Airborne Contamination 0 7/98 Survey Report Form Scaler Setup Sheet 0 7/98 Scaler Daily Source Check Sheet 0 7/98 SOP 29.1 None SOP 30.1 None SOP 31.1 None SOP 32.1 Surface Contamination Values 1 3/99 Guidelines for Contamination Control 1 3/99 Practices Guidelines for Contamination Control 1 3/99 Practices J:\DOE\4000\D3\SQ&OPS\WASOPS\SOP_TOC1299.DOC WEISS ASSOCIATES Project Number: 128-4000 Standard Operating Procedures and Forms Table of Contents LEHR Environmental Restoration / Waste Management 12/10/99 DOE Contract No. DE-AC03-96SF20686 Page v of vi Checklist for Reducing Occupational 1 3/99 Radiation Exposure Physical Access Controls for High and 1 3/99 Very High Radiation Areas Guidelines for Personnel Contamination 1 3/99 Monitoring with Hand Held Instruments SOP 34.1 Container Log 0 3/98 SOP 34.2 Waste Management Weekly Inspection Checklist SOP 34.3 Waste Shipment Checklist 0 7/98 Transport Vehicle Inspection Checklist 0 7/98 Exclusive Use Instructions 0 7/98 Document Package Distribution 0 7/98 SOP 34.4 Waste/Material Evaluation Process 2 6/01 SOP 34.5 Example of Waste Tracking Sheet (Form 0 2/99 SOP 34.5) Example of Completed Waste Tracking 0 2/99 Sheet SOP 35.1 None SOP 37.1 None SOP 37.2 None SOP 38.1 LEHR Visitor Sign-In Log 2 11/99 Visitor Orientation Form 2 11/99 General Employee Radiation Training Log 2 11/99 (GERT) Personal/Occupational History 2 11/99 Request for Report of Radiation History 2 11/99 Training Certificate List 2 11/99 SOP 38.2 None SOP 38.3 None SOP 38.4 RPP Audit Plan Schedule 1 3/99 SOP 38.5 None SOP 39.1 None SOP 40.1 Environmental Dosimetry Inspection Form 0 4/98 TLD Locations 0 11/97 SOP 41.1 QA/QC Checklist for Documents 0 3/98 Document Review Tracking Form 0 3/98 SOP 42.1 US DOE Individual Accident/Incident Report DOE M 32.1-1 Tabulation of Work Hours and Vehicle Usage, and Property Valuation J:\DOE\4000\D3\SQ&OPS\WASOPS\SOP_TOC1299.DOC WEISS ASSOCIATES Project Number: 128-4000