इंटरनेट मानक Disclosure to Promote the Right To Information Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public. “जान1 का अ+धकार, जी1 का अ+धकार” “प0रा1 को छोड न’ 5 तरफ” Mazdoor Kisan Shakti Sangathan Jawaharlal Nehru “The Right to Information, The Right to Live” “Step Out From the Old to the New” IS 1388-2 (2005): Laboratory Glassware - Bottles, Part 2: Conical Nec Bottles [CHD 10: Glassware] “!ान $ एक न’ भारत का +नम-ण” Satyanarayan Gangaram Pitroda ““IInnvveenntt aa NNeeww IInnddiiaa UUssiinngg KKnnoowwlleeddggee”” “!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता हहहहै””ै” Bhartṛhari—Nītiśatakam “Knowledge is such a treasure which cannot be stolen” IS 1388 (Part 2) :2005 ISO 4796-2:2000 W@v7Fm \ +iJlqm5-mm –M Wilwlldf m2?kKmT?+rvim$i (v !p-$$m ) Indian Standard LABORATORY GLASSWARE — BOTTLES PART 2 CONICAL NECK BOTTLES Second Revision ( ICS 71.040.20 @BIS 2005 BUREAU OF INDIAN STANDARDS MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG NEW DELHI 110002 Price Group 3 June 2005 Glass, Glassware and Laboratoryware Sectional Committee, CHD 10 NATIONAL FOREWORD This Indian Standard (Part 2) (Second Revision) which is identical with ISO 4796-2:2000 ‘Laboratory glassware — Bottles — Part 2: Conical neck bottles’ issued by the International Organization for Standardization (ISO) was adopted by the Bureau of Indian Standards on the recommendations of the Glass, Glassware and Laboratoryware Sectional Committee and approval of the Chemical Division Council. IS 1388:1993 ‘Reagent bottles (first revision)’ was first published inl 959 and revised in 1993. During second revision, the Committee felt that it would be more convenient to split the standard into three parts by adoption of ISO 4796-1 :2000, ISO 4796-2:2000 and ISO 4796-3:2000 on dual number basis. Part 1 covered Screw-neck bottles, Part 2 covered Conical neck bottles and Part 3 covered Aspirator bottles. The text of this ISO Standard has been proposed to be approved as suitable for publication as an Indian Standard without deviations. Certain conventions are, however, not identical to those used in Indian Standards. Attention is particularly drawn to the following: a) Wherever the words ‘International Standard’ appear referring to this standard, they should be read as ‘Indian Standard’. b) Comma (,) has been used as adecimal marker while in Indian Standards, the current practice is to use a point (.) as the decimal marker. BIS Certification Marking clause is given in National Annex A. Inthis adopted standard, reference appears to certain International Standards for which Indian Standards also exist. The corresponding Indian Standards which are to be substituted in their places are listed below along with their degree of equivalence for the editions indicated: International Standard Corresponding Indian Standard Degree of Equivalence ISO 383:1976 Laboratory gla ss- IS 5165: 1969 Interchangeable conical Equivalent ware — Interchangeable conical ground-glass joints ground joints 1s0 719 : 1985 Glass — IS2313 (Part l/See 1): 1994 Grading glass do Hydrolytic resistance of glass alkalinity: Part 1 Hydrolytic resistartce, grains at 98°C — Method of test Section 1 Hydrolytic resistance of g~ass and classification grains at 98°C — Method of test and ,“ classification ISO 4796-1 : 2000 Laboratory IS 1388 (Part 1) : 2005 Laboratory Identical glassware — Bottles — Part 1 : glassware — Bottles : Part 1 Screw-neck Screw-neck bottles bottles The Technical Committee responsible for the preparation of this standard has reviewed the provisions of the following International Standard and has decided that the same is acceptable for use in conjunction with this standard: International Standard Title ISO 3585:1998 Borosilicate glass 3.3- Properties (Continued on third cover) IS 1388 (Part 2) :2005 ISO 4796-2:2000 Indian Standard LABORATORY GLASSWARE — BOTTLES PART 2 CONICAL NECK BOTTLES Second Revision) ( 1 Scope This part of ISO 4796 specifies a series of bottles with a conical, wide or narrow neck with or without ground joints, suitable for the storage of liquid and solid chemicals and reagents in general laboratory use. 2 Normative references The following normative documents contain provisions which, through reference in this text, constitute provisions of this parl of ISO 4796. For dated references, subsequent amendments to, or revisions of, any of these publications do not apply. However, parties to agreements based on this part of ISO 4796 are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition of the normative document referred to applies. Members of ISO and IEC maintain registers of currently valid International Standards. ISO 383:1976, Laboratory glassware — Interchangeable conical ground joints. ISO 719:1985, Glass — Hydrolytic resistance of glass grains at 98 “C — Method of test and classification. ISO 3585:1998, Borosilicate glass 3.3 — Propetiies. ISO 4796-1:2000, Laboratory glassware — Bottles — Part 1:Screw-neck bottles. ‘ 3 Types and capacities 3.1 There are four types of conical neck bottles specified inthis part of ISO 4796: — type WS: wide-necked bottles with a conical socket; type WJ: wide-necked bottles with an interchangeable conical ground joint; — type NS: narrow-necked bottles with a conical socket; ,$ — type NJ: narrow-necked bottles with an interchangeable conical ground joint. J 3.2 The nominal capacities of conical neck bottles shall be-chosen from the following series: — wide-necked bottles: 50 ml — 100 ml — 250 ml — 500 ml — 1000 ml and 2000 ml; — narrow-necked bottles: 25 ml — 30 ml — 50 ml — 100 ml — 250 ml — 500 ml — 1000 ml — 2000 ml — 2500 ml — 5000 ml — 10000 ml and 20000 ml. 1 IS 1388 (Part 2) :2005 ISO 4796-2:2000 3.3 The nominal capacity of a bottle indicates the quantity of liquid which a bottle of average wall thickness shall contain when the bottle isfilled to the turn of the shoulder. 3.4 The design of the bottle shall be such that the total capacity to the base of the neck shall be approximately 15 % greater than that to the shoulder. 4 Dimensions The dimensions and tolerances of conical neck bottles are given in Figures 1and 2 and in Table 1. Table 1— Dimensions Nominal Total Outside Wall Recommended capacity height diameter thickness socket/ground joint a h d s ml mm mm mm wide neck narrow neck approx. approx. min. 25 64 36 1,0 — 12/21 30 78 36 1,0 — 16/16 50 78 42 1,0 24/20 14115 100 95 52 1,2 29/22 14/15 or 14/23 250 128 70 1,3 34/35 19/22 or 19/26 500 162 86 1,3 45/40 24/29 1000 198 107 1,7 60/46 29/32 2000 246 133 2,0 60/46 29/32 2500 295 140 2,0 — 24/20 5000 318 181 2,0 — 45/40 10000 398 227 2,7 — 60/46 20000 492 288 3,0 — 60/46 ]Inaccordance with ISO383 (see5.2.8fordetails) 5 Construction 5.1 Material 5.1.1 Bottles with conical necks shall be constructed of clear, colorless or amber borosilicate glass 3.3 in accordance with ISO 3585 or from other glass types, complying with the requirements of class HGB-3 or better specified in ISO 719. 5.1.2 Internal stress and visible defects in the glass (such as bubbles near the surface) shall be reduced to a level sufficient to minimize the possibility of fracture due to thermal or mechanical shock. 5.2 Design 5.2.1 The base of the bottle shall be constructed so as to enable the bottle to stand firmly on a flat surface without rocking or spinning. 2 IS 1388 (Part 2) :2005 ISO 4796-2:2000 1“ I -c 2 s / --J — @d l-= @d Key Key 1 Taper l:10 1 Taper l:10 2 Taper 1:30 2 Taper 1:30 Figure 1— Wide-necked bottle Figure 2 — Narrow-necked bottle 5.2.2 The base of the bottle shall have a suitable radius so as to provide a smooth transition between the base and the side. The main portion of the side shall be slightly tapered with the smaller diameter at the base of the bottle. The diameters dand the heights hshall be as given in Table 1. 5.2.3 The shoulder of the bottle shall have a suitable radius in order to provide a smooth transition between the side and the conical upper proportion of the bottle. 5.2.4 The upper portion of the shoulder shall be of conical shape. The transition radius from the upper portion of the shoulder to the neck shall be as small as possible to be compatible with good manufacturing practice. 5.2.5 The bottle shall be blown so as to evenly distribute the glass in the mould avoiding sudden changes in the wall thickness, The thinnest areas shall not have athickness less than the minimum values specified in Table 1. 3 IS 1388 (Part 2) :2005 ISO 4796-2:2000 5.2.6 The neck of the bottle shall be stoutly constructed and finished with a strengthening lip designed to facilitate pouring without liquid running down the outside of the bottle. 5.2.7 The outer glass surface of the bottles maybe coated with a suitable plastics material as a protection and to limit leakage of liquid ifthe bottle is damaged. The coating shall be resistant to steam sterilization at 135 “C. 5.2.8 The internal surface of the conical neck socket shall be smooth, suitable to fit with a rubber stopper, or shall be finished by fine grinding. If the surface is finished, the grinding shall comply with the interchangeable conical ground joints specified in ISO 383 and with the dimensions specified in Table 1 of this part of ISO 4796. If the socket surface is smooth, the socket dimensions shall be suited for finishing by fine grinding so as to fit an interchangeable conical ground joint specified in Table 1. 5.3 Stoppers 5.3.1 Bottles shall be provided with stoppers of glass, rubber or of a suitable inert plastics material. 5.3.2 Glass stoppers shall be made of glass of a similar coefficient of thermal expansion to that of the bottle. The glass stoppers shall be ground to ajoint complying with the requirements of ISO 383 and they shall comply with the sizes given in Table 1. 5.3.3 Rubber stoppers shall be dimensioned to fit with the conical smooth socket of the bottle neck, given in Table 1. 5.3.4 Plastics stoppers shall be made from a suitable inert material, for example polypropylene or polyethylene, and shall be moulded to fit with the interchangeable conical ground joint of the bottle neck. 5.3.5 Glass or plastic stoppers should have a flat top with a grip, larger than the diameter of the lip of the neck with which they are intended to be used. The grip shall facilitate removal of the stopper from the neck of the bottle, for example by being of a hexagonal or similar shape. 6 Designation If a designation of bottles is required, this shall be by reference to this part of ISO 4796, i.e. ISO 4796-2, together with the nominal capacity and the type specified in 3.1. EXAMPLE For a bottle with a nominal capacity of 100 ml and of type WS (wide-necked bottle with a conical socket), the designation would be as follows: Laboratory bottle ISO4796-2-100 WS 7 Marking ,, In accordance with ISO 4796-1:2000. 4 IS 1388 (Part 2) :2005 ISO 4796-2:2000 NATIONAL ANNEX A (National Foreword) A-1 BIS CERTIFICATION MARKING The product may also be marked with the Standard Mark. A-1.1 The use of the Standard Mark isgoverned bythe provisions ofthe Bureau of hdian Standards Act, 1986 and the Rules and Regulations made thereunder. The details of conditions under which the Iicence for the use of Standard Mark may be granted to manufacturers or producers may be obtained from the Bureau of Indian Standards. 5